| Abstract: | A method is described for the analysis of polychlorinated biphenyl (PCB) compounds in tissue samples. Cleanup by hexane-aceto-nitrile partitioning and Florisil column chromatography are performed on samples before oxidative treatment to convert DDE to DCBP. PCB components are then determined semi-quantitatively by TLC. No prior separation of PCB from chlorinated pesticides is required. The lower limit of sensitivity is 0.2 ?g. |
| Genre: | Article |
| ProdID: | 5221236 |
| Citation Author: | Mulhern, B.M; Cromartie, E.; Reichel, W.L; Belisle, A.A. |
| Citation Contributing Office: | Patuxent Wildlife Research Center |
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| Citation End Page: | 550 |
| Citation Issue: | 3 |
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| Citation Language: | English |
| Citation Larger Work Title: | Journal of the Association of Official Analytical Chemists |
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| Citation Number Of Pages: | 3 |
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| Citation Phsyical Description: | 548-550 |
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| Citation Search Results Text: | Semiquantitative determination of polychlorinated biphenyls in tissue samples by thin layer chromatography; 1971; Article; Journal; Journal of the Association of Official Analytical Chemists; Mulhern, B.M; Cromartie, E.; Reichel, W.L; Belisle, A.A. |
| Citation Start Page: | 548 |
| Citation Volume: | 54 |
| Citation Year: | 1971 |
| Type: | citation/reference |
| Text: | Semiquantitative determination of polychlorinated biphenyls in tissue samples by thin layer chromatography; 1971; Article; Journal; Journal of the Association of Official Analytical Chemists; Mulhern, B.M; Cromartie, E.; Reichel, W.L; Belisle, A.A. |
| URL (THUMBNAIL): | http://pubs.er.usgs.gov/thumbnails/outside_thumb.jpg |
| Date Other: | Wed, 16 Jun 2010 12:17 -0500 |
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