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Nuclear magnetic resonance studies of the phosphorus(v) pesticides. A rapid determination of the isomer ratio of systox1 1 Publication authorised by the Director U.S. Geological Survey.

Analytica Chimica Acta

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Abstract

The integration circuit of the Varian A-60 nuclear magnetic resonance spectrometer is used in conjunction with vapor phase chromatography, to develop a rapid analysis technique for the determination of isomer ratios in technical Systox-Sulfotepp mixtures. The complete analysis requires less than 0.1 g of sample and only 15 min. The isomer ratio in the sample may be determined to an accuracy of ??1.5% and the undamaged sample may be recovered. ?? 1968.

Additional Publication Details

Publication type:
Article
Publication Subtype:
Journal Article
Title:
Nuclear magnetic resonance studies of the phosphorus(v) pesticides. A rapid determination of the isomer ratio of systox1 1 Publication authorised by the Director U.S. Geological Survey.
Series title:
Analytica Chimica Acta
Volume
40
Issue:
C
Year Published:
1968
Language:
English
Larger Work Type:
Article
Larger Work Subtype:
Journal Article
Larger Work Title:
Analytica Chimica Acta
First page:
387
Last page:
392
Number of Pages:
6