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Formation of hydrogen peroxide in the silver reductor: A micro-analytical method for iron

Journal of the American Chemical Society

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Abstract

1. An attempt to determine small quantities of iron by reduction with silver followed by titration with eerie sulfate revealed an error attributable to the formation of hydrogen peroxide in the reductor. 2. By conducting the reduction in an atmosphere of hydrogen, thereby decreasing the reductor correction, and applying a correction for the indicator, it was possible to determine quantities of iron of the order of 1.5 mg. with a high degree of accuracy. 3. The method was found to be relatively rapid and not to require the use of large platinum dishes, thus possessing advantages of practical value.

Additional Publication Details

Publication type:
Article
Publication Subtype:
Journal Article
Title:
Formation of hydrogen peroxide in the silver reductor: A micro-analytical method for iron
Series title:
Journal of the American Chemical Society
Volume
58
Issue:
5
Year Published:
1936
Language:
English
Larger Work Type:
Article
Larger Work Subtype:
Journal Article
Larger Work Title:
Journal of the American Chemical Society
First page:
826
Last page:
831