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Determination of rare earth elements in geological materials by inductively coupled argon plasma/atomic emission spectrometry

Analytical Chemistry

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Abstract

Inductively coupled argon plasma/optical emission spectrometery (ICAP/OES) is useful as a simultaneous, multielement analytical technique for the determination of trace elements in geological materials. A method for the determination of trace-level rare earth elements (REE) in geological materials using an ICAP 63-channel emission spectrometer is described. Separation and preconcentration of the REE and yttrium from a sample digest are achieved by a nitric acid gradient cation exchange and hydrochloric acid anion exchange. Precision of 1-4% relative standard deviation and comparable accuracy are demonstrated by the triplicate analysis of three splits of BCR-1 and BHVO-1. Analyses of other geological materials including coals, soils, and rocks show comparable precision and accuracy.

Additional Publication Details

Publication type:
Article
Publication Subtype:
Journal Article
Title:
Determination of rare earth elements in geological materials by inductively coupled argon plasma/atomic emission spectrometry
Series title:
Analytical Chemistry
Volume
54
Issue:
8
Year Published:
1982
Language:
English
Larger Work Type:
Article
Larger Work Subtype:
Journal Article
Larger Work Title:
Analytical Chemistry
First page:
1329
Last page:
1332
Number of Pages:
4