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Extraction and speciation of arsenic in lacustrine sediments

Talanta

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Abstract

Arsenic was partially extracted with 4.OM hydrochloric acid, from samples collected at 25-cm intervals in a 350-cm column of sediment at Milltown Reservoir, Montana and from a 60-cm core of sediment collected at the Cheyenne River Embayment of Lake Oahe, South Dakota. The sediment in both reservoirs is highly contaminated with arsenic. The extracted arsenic was separated into As(III) and As(V) on acetate form Dowex 1-X8 ion-exchange resin with 0.12M HCl eluent. Residual arsenic was sequentially extracted with KClO3 and HCl. Arsenic was determined by graphite-furnace atomic-absorption spectrometry. The analytical results define oxidized and reduced zones in the sediment columns. ?? 1990.

Additional Publication Details

Publication type:
Article
Publication Subtype:
Journal Article
Title:
Extraction and speciation of arsenic in lacustrine sediments
Series title:
Talanta
Volume
37
Issue:
8
Year Published:
1990
Language:
English
Larger Work Type:
Article
Larger Work Subtype:
Journal Article
Larger Work Title:
Talanta
First page:
831
Last page:
834
Number of Pages:
4