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A short working distance multiple crystal x-ray spectrometer

Review of Scientific Instruments

By:
, , , , , , ,
DOI: 10.1063/1.3048544

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Abstract

For x-ray spot sizes of a few tens of microns or smaller, a millimeter-sized flat analyzer crystal placed ???1 cm from the sample will exhibit high energy resolution while subtending a collection solid angle comparable to that of a typical spherically bent crystal analyzer (SBCA) at much larger working distances. Based on this observation and a nonfocusing geometry for the analyzer optic, we have constructed and tested a short working distance (SWD) multicrystal x-ray spectrometer. This prototype instrument has a maximum effective collection solid angle of 0.14 sr, comparable to that of 17 SBCA at 1 m working distance. We find good agreement with prior work for measurements of the Mn K?? x-ray emission and resonant inelastic x-ray scattering for MnO, and also for measurements of the x-ray absorption near-edge structure for Dy metal using L??2 partial-fluorescence yield detection. We discuss future applications at third- and fourth-generation light sources. For concentrated samples, the extremely large collection angle of SWD spectrometers will permit collection of high-resolution x-ray emission spectra with a single pulse of the Linac Coherent Light Source. The range of applications of SWD spectrometers and traditional multi-SBCA instruments has some overlap, but also is significantly complementary. ?? 2008 American Institute of Physics.

Additional Publication Details

Publication type:
Article
Publication Subtype:
Journal Article
Title:
A short working distance multiple crystal x-ray spectrometer
Series title:
Review of Scientific Instruments
DOI:
10.1063/1.3048544
Volume
79
Issue:
12
Year Published:
2008
Language:
English
Larger Work Type:
Article
Larger Work Subtype:
Journal Article