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A multi-residue method for the analysis of pesticides and pesticide degradates in water using HLB solid-phase extraction and gas chromatography-ion trap mass spectrometry

Bulletin of Environmental Contamination and Toxicology

By:
, , and
DOI: 10.1007/s00128-007-9332-2

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Abstract

A method was developed for the analysis of over 60 pesticides and degradates in water by HLB solid-phase extraction and gas-chromatography/mass spectrometry. Method recoveries and detection limits were determined using two surface waters with different dissolved organic carbon (DOC) concentrations. In the lower DOC water, recoveries and detection limits were 80%-108% and 1-12 ng/L, respectively. In the higher DOC water, the detection limits were slightly higher (1-15 ng/L). Additionally, surface water samples from four sites were analyzed and 14 pesticides were detected with concentrations ranging from 4 to 1,200 ng/L. ?? 2008 Springer Science+Business Media, LLC.

Additional Publication Details

Publication type:
Article
Publication Subtype:
Journal Article
Title:
A multi-residue method for the analysis of pesticides and pesticide degradates in water using HLB solid-phase extraction and gas chromatography-ion trap mass spectrometry
Series title:
Bulletin of Environmental Contamination and Toxicology
DOI:
10.1007/s00128-007-9332-2
Volume
80
Issue:
2
Year Published:
2008
Language:
English
Larger Work Type:
Article
Larger Work Subtype:
Journal Article
Larger Work Title:
Bulletin of Environmental Contamination and Toxicology
First page:
139
Last page:
144
Number of Pages:
6