A multi-residue method for the analysis of pesticides and pesticide degradates in water using HLB solid-phase extraction and gas chromatography-ion trap mass spectrometry
Bulletin of Environmental Contamination and Toxicology
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Abstract
A method was developed for the analysis of over 60 pesticides and degradates in water by HLB solid-phase extraction and gas-chromatography/mass spectrometry. Method recoveries and detection limits were determined using two surface waters with different dissolved organic carbon (DOC) concentrations. In the lower DOC water, recoveries and detection limits were 80%–108% and 1–12 ng/L, respectively. In the higher DOC water, the detection limits were slightly higher (1–15 ng/L). Additionally, surface water samples from four sites were analyzed and 14 pesticides were detected with concentrations ranging from 4 to 1,200 ng/L.
| Publication type | Article |
|---|---|
| Publication Subtype | Journal Article |
| Title | A multi-residue method for the analysis of pesticides and pesticide degradates in water using HLB solid-phase extraction and gas chromatography-ion trap mass spectrometry |
| Series title | Bulletin of Environmental Contamination and Toxicology |
| DOI | 10.1007/s00128-007-9332-2 |
| Volume | 80 |
| Issue | 2 |
| Year Published | 2008 |
| Language | English |
| Publisher | Springer |
| Contributing office(s) | California Water Science Center, Toxic Substances Hydrology Program |
| Description | 6 p. |
| First page | 139 |
| Last page | 144 |
| Google Analytic Metrics | Metrics page |